The Powder Materials Laboratory at IIT


Powder Characterization | Synthesis | Consolidation | Sintering | Testing | Modeling | Research Affiliates | Educational Programs | Industrial Advisory Board | Clients | Staff | Recent Theses | Further Information

Powder metallurgy (P/M) offers a highly reliable, cost-effective way of manufacturing ferrous and non ferrous parts ranging from tool and die materials to oil-impregnated bushings. Because P/M parts can be produced at-or very close to-final dimensions and can be coined or forged for higher density and strength than parts manufactured conventionally, P/M is in many applications a superior process. It is also an energy and materials conserving process. P/M typically uses 97 percent of the starting raw material in the finished part. Global competition that has stimulated parts manufacturers to focus on improving quality and reducing manufacturing costs has stimulated an increase in the use of powder metallurgy and spurred advances in the field. The Powder Materials Laboratory at Illinois Institute of Technology offers a resource for keeping abreast of changes, developing and testing materials for specific applications, developing and modifying technology, manufacturing prototype or special parts, and developing or enhancing your knowledge base in the field.

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A resource in research and education
Since its inception in 1986, the Powder Materials Laboratory at IIT has been involved in research for the powder metallurgy industry and in education of students in this growing field. A number of our graduates are now working directly in the powder metallurgy industry, while others are involved in P/M research. The well-equipped laboratory has been enhanced in recent years with an investment of $1,000,000 in equipment. Through our Powder Materials Laboratory, which is part of the Manufacturing Center at IIT, we make a broad range of equipment and expertise available to manufacturers. Laboratory capabilities include:
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Powder Characterization
True powder density by helium pycnometer
Surface area by multipoint BET analysis
Thermogravimetric analysis
Particle size distribution by sieve analysis and centrifugal sedimentation apparatus
Apparent density, tap density and flow rate
Compressibility
Sampling by sieving riffler
Powder morphology by scanning electron microscopy
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 Synthesis
 
Mechanical alloying in batch quantities from 1 gram to 1 kg

    using SPEX or Union Process mills..
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Consolidation
A 4 ton automatic cold die press
2 50 ton platen presses
A 1200C, 120 MPa hot press
A 210 MPa cold isostatic press (6"x24" chamber)
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Sintering
40' pusher sintering furnace with hydrogen/nitrogen atmosphere control system
Laboratory scale vacuum and controlled atmosphere furnaces
Vacuum induction furnace
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Consolidated Property Testing
Green density, green strength
Sintered strength by 3-point bend and tensile tests
Microhardness
Impact and fatigue tests
Pore and grain size and distribution by optical and scanning electron microscopy
Retained austenite, texture and phase analysis by X-ray diffraction
Chemical analysis by energy dispersive spectrometry

MPIF Standard Test Methods:

02, 03, 04, 05, 10, 15, 28, 40, 41, 43, 44, 45, 46, 49 51, 52, 53
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Modeling
Hot isostatic pressing
Thermodynamic modeling of sintering
Finite element analysis: stress analysis of parts; analysis of compaction process
Heat transfer modeling
Magnetic field modeling
Diffusion modeling
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Research Affiliates program

IIT Powder Metallurgy Laboratory affiliates ($1,000 annual dues) qualify for the following benefits:

Discounts on contract research fees
Access to library information services (includes 2 computerized literature searches)
Annual report of the Powder Materials Laboratory containing detailed reports of non-proprietary research performed
Advance information about new courses
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Educational Program

Our education program includes regular undergraduate IIT courses such as Powder Metallurgy (METM 413), Powder Metallurgy Laboratory (METM 416) and Composites (METM 475); other courses relevant to P/M technology and materials analysis, short courses, and review courses for the powder materials certification exams.
IIT has recently introduced the Interprofessional Projects Program as part of our undergraduate curricculum. This program provides a real-world project-based team experience with balanced company and faculty mentoring. For information on how your company can participate in this program contact Professor Philip Nash.

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Industrial Advisory Board The Industrial Advisory Board is made up of several people from local companies. The purpose of the advisory board is to provide input to all aspects of the Powder Materials Program from an industrial viewpoint. Members of the PM Industrial Advisory Board are:
Herman Amaya-MIMTEC
Steve Constantinides-The Arnold Engineering Company
Peter dePoutelieff-SSI Technologies
Chaman Lall- Sintered Metals-Chicago
Tom Prucher-Burgess Norton Manufacturing Company
Chuck Rose-Bronson & Bratton
Jack Webster-Webster-Hoff
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Clients

Companies and government agencies we have done or are doing P/M research or consulting for include:

Advance Products
Air Force Office of Scientific Research
Air Liquide
American Institute of Biotechnology
Argonne National Laboratory
The Arnold Engineering Company
Brezina & Ehrlich
Danly Engineering
General Motors
Inductametals
Los Alamos National Laboratory
Magnetics International
Sintered Metals-Chicago Inc.
MIMTEC
National Waste Recovery Systems Inc.
Timing Gears Corp.
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Staff

Director of the Powder Materials Laboratory, Philip Nash, Ph.D., is a professor of metallurgical and materials engineering at IIT who teaches P/M lecture and laboratory courses. An active researcher as well as teacher, Professor Nash has served as a research adviser to dozens of graduate students, and has been an instructor in MPIF short courses and helped organize international P/M conferences. He is a member of the APMI and a consultant for industry. Finite Element Modeling is performed by Guiru Liu Nash, who is a consultant in this area to industry.

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Recent theses in P/M area
P. Khedkar, "Evaluation of Cooling Rate & Hot Pressing of Rapidly Solidified U700"
S.N. Patel, "The Effect of Type and Particle Size Distribution of Iron Powders on Compressibility"
A. Patel, "Processing and Mechanical Properties of Particulate and Fiber Reinforced Intermetallic (B2 NiAl) Matrix Composites"
P. Desch, "Synthesis of Trialuminides by Mechanical Alloying"
N. Dillinger "Processing Parameters for Mechanical Alloying Using a Triple Arm Attritor Mill"
S.J. Hwang, "The Microstructure and Mechanical Properties of Mechanically Alloyed NiAl-based Alloys"
R. Bielinda "Control of Sintering Atmospheres Using Thermodynamic Calculations"
H. Ardy "Consolidation of Mechanically Alloyed Intermetallic Powders"
S. Wu "Synthesis of Composite Intermetallic Powders by Mechanical Alloying"
H. Kim, "A Study of Mechanically Alloyed Titanium Aluminides"
H. Choo, "Synthesis of Mechanically Alloyed NiAl/Alumina composites."
C.J. Wen, "The Influence of Sintering Atmospheres and Boron additions on the Sintering and Mechanical Properties of FCO208."
S. C. Ur, "Secondary Recrystallization and Grain Growth in Mechanically Alloyed NiAl"
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For further information

For information on how you can use IIT's P/M resources please call, write, e-mail or fax
Professor Philip Nash
Department of Mechanical, Materials and Aerospace Engineering,
Illinois Institute of Technology
10 West 32nd St., Room 238
Chicago, IL 60616-3793

Telephone: (312) 567-3056 Fax: (312) 567-8875


nash@charlie.iit.edu
 

Powder Characterization | Synthesis | Consolidation | Sintering | Testing | Modeling | Research Affiliates | Educational Programs | Industrial Advisory Board | Clients | Staff | Recent Theses | Further Information

 
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Last update: February 8th 1998.