The Powder Materials
Laboratory at IIT
Powder Characterization | Synthesis
| Consolidation | Sintering
| Testing | Modeling | Research
Affiliates | Educational Programs | Industrial
Advisory Board | Clients | Staff
| Recent Theses | Further Information
Powder metallurgy (P/M) offers a highly reliable, cost-effective way
of manufacturing ferrous and non ferrous parts ranging from tool and die
materials to oil-impregnated bushings. Because P/M parts can be produced
at-or very close to-final dimensions and can be coined or forged for higher
density and strength than parts manufactured conventionally, P/M is in
many applications a superior process. It is also an energy and materials
conserving process. P/M typically uses 97 percent of the starting raw material
in the finished part. Global competition that has stimulated parts manufacturers
to focus on improving quality and reducing manufacturing costs has stimulated
an increase in the use of powder metallurgy and spurred advances in the
field. The Powder Materials Laboratory at Illinois Institute of Technology
offers a resource for keeping abreast of changes, developing and testing
materials for specific applications, developing and modifying technology,
manufacturing prototype or special parts, and developing or enhancing your
knowledge base in the field.
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A resource in research and education
Since its inception in 1986, the Powder Materials Laboratory at IIT
has been involved in research for the powder metallurgy industry and in
education of students in this growing field. A number of our graduates
are now working directly in the powder metallurgy industry, while others
are involved in P/M research. The well-equipped laboratory has been enhanced
in recent years with an investment of $1,000,000 in equipment. Through
our Powder Materials Laboratory, which is part of the Manufacturing Center
at IIT, we make a broad range of equipment and expertise available to manufacturers.
Laboratory capabilities include:
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Powder Characterization
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True powder density by helium
pycnometer
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Surface area by multipoint
BET analysis
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Thermogravimetric analysis
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Particle size distribution
by sieve analysis and centrifugal
sedimentation apparatus
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Apparent density, tap density
and flow rate
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Compressibility
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Sampling by sieving riffler
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Powder morphology by scanning
electron microscopy
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Synthesis
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Mechanical alloying in batch
quantities from 1 gram to 1 kg
using SPEX or Union Process mills..
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Consolidation
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A 4 ton automatic cold die
press
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2 50 ton platen presses
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A 1200C, 120 MPa hot press
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A 210 MPa cold
isostatic press (6"x24" chamber)
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Sintering
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40' pusher sintering furnace
with hydrogen/nitrogen atmosphere control system
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Laboratory scale vacuum and
controlled atmosphere furnaces
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Vacuum
induction furnace
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Consolidated Property Testing
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Green density, green strength
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Sintered strength by 3-point
bend and tensile tests
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Microhardness
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Impact and fatigue tests
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Pore and grain size and distribution
by optical and scanning electron microscopy
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Retained austenite, texture
and phase analysis by X-ray diffraction
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Chemical analysis by energy
dispersive spectrometry
MPIF Standard Test Methods:
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02, 03, 04, 05, 10, 15, 28,
40, 41, 43, 44, 45, 46, 49 51, 52, 53
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Modeling
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Hot isostatic pressing
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Thermodynamic modeling of sintering
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Finite element analysis: stress
analysis of parts; analysis of compaction process
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Heat transfer modeling
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Magnetic field modeling
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Diffusion modeling
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Research Affiliates program
IIT Powder Metallurgy Laboratory affiliates ($1,000 annual dues) qualify
for the following benefits:
-
Discounts on contract research
fees
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Access to library information
services (includes 2 computerized literature searches)
-
Annual report of the Powder
Materials Laboratory containing detailed reports of non-proprietary research
performed
-
Advance information about new
courses
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Educational Program
Our education program includes regular undergraduate IIT courses such
as Powder Metallurgy (METM 413), Powder Metallurgy Laboratory (METM 416)
and Composites (METM 475); other courses relevant to P/M technology and
materials analysis, short courses, and review courses for the powder materials
certification exams.
IIT has recently introduced the Interprofessional Projects Program
as part of our undergraduate curricculum. This program provides a real-world
project-based team experience with balanced company and faculty mentoring.
For information on how your company can participate in this program contact
Professor Philip Nash.
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Industrial Advisory Board The Industrial
Advisory Board is made up of several people from local companies. The purpose
of the advisory board is to provide input to all aspects of the Powder
Materials Program from an industrial viewpoint. Members of the PM Industrial
Advisory Board are:
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Herman Amaya-MIMTEC
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Steve Constantinides-The Arnold Engineering Company
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Peter dePoutelieff-SSI Technologies
-
Chaman Lall- Sintered Metals-Chicago
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Tom Prucher-Burgess Norton Manufacturing Company
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Chuck Rose-Bronson & Bratton
-
Jack Webster-Webster-Hoff
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Clients
Companies and government agencies we have done or are doing P/M research
or consulting for include:
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Advance Products
-
Air Force Office of Scientific
Research
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Air Liquide
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American Institute of Biotechnology
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Argonne National Laboratory
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The Arnold Engineering Company
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Brezina & Ehrlich
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Danly Engineering
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General Motors
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Inductametals
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Los Alamos National Laboratory
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Magnetics International
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Sintered Metals-Chicago Inc.
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MIMTEC
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National Waste Recovery Systems Inc.
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Timing Gears Corp.
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Staff
Director of the Powder Materials Laboratory, Philip
Nash, Ph.D., is a professor of metallurgical and materials engineering
at IIT who teaches P/M lecture and laboratory courses. An active researcher
as well as teacher, Professor Nash has served as a research adviser to
dozens of graduate students, and has been an instructor in MPIF short courses
and helped organize international P/M conferences. He is a member of the
APMI and a consultant for industry. Finite Element Modeling is performed
by Guiru Liu Nash, who is a consultant
in this area to industry.
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Recent theses in P/M area
-
P. Khedkar, "Evaluation of
Cooling Rate & Hot Pressing of Rapidly Solidified U700"
-
S.N. Patel, "The Effect of
Type and Particle Size Distribution of Iron Powders on Compressibility"
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A. Patel, "Processing and Mechanical
Properties of Particulate and Fiber Reinforced Intermetallic (B2 NiAl)
Matrix Composites"
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P. Desch, "Synthesis of Trialuminides
by Mechanical Alloying"
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N. Dillinger "Processing Parameters
for Mechanical Alloying Using a Triple Arm Attritor Mill"
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S.J.
Hwang, "The Microstructure and Mechanical Properties of Mechanically
Alloyed NiAl-based Alloys"
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R. Bielinda "Control of Sintering
Atmospheres Using Thermodynamic Calculations"
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H. Ardy "Consolidation of Mechanically
Alloyed Intermetallic Powders"
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S. Wu "Synthesis of Composite
Intermetallic Powders by Mechanical Alloying"
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H. Kim,
"A Study of Mechanically Alloyed Titanium Aluminides"
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H.
Choo, "Synthesis of Mechanically Alloyed NiAl/Alumina composites."
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C.J. Wen, "The Influence of
Sintering Atmospheres and Boron additions on the Sintering and Mechanical
Properties of FCO208."
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S. C.
Ur, "Secondary Recrystallization and Grain Growth in Mechanically Alloyed
NiAl"
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For further information
For information on how you can use IIT's P/M resources please call,
write, e-mail or fax
Professor Philip Nash
Department of Mechanical, Materials and Aerospace Engineering,
Illinois Institute of Technology
10 West 32nd St., Room 238
Chicago, IL 60616-3793
Telephone: (312) 567-3056 Fax: (312) 567-8875
nash@charlie.iit.edu
Powder Characterization | Synthesis
| Consolidation | Sintering
| Testing | Modeling | Research
Affiliates | Educational Programs | Industrial
Advisory Board | Clients | Staff
| Recent Theses | Further Information
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Last update: February 8th 1998.